Scientific American Supplement, No. 275, April 9, 1881

CEREALINE.–The cells composing the embryous membrane contain, as already stated, the cerealine, but after the germination they contain cerealine and diastase, that is to say, a portion of the cerealine changed into diastase, with which it has the greatest analogy. It is known how difficult it is to isolate and study albuminous substances. The following is the method of obtaining and studying cerealine. Take the raw embryous membrane, prepared as stated, steep it for an hour in spirits of wine diluted with twice its volume of water, and renew this liquid several times until the dextrine, glucose, coloring matters, etc., have been completely removed. The membranes should now be pressed and cast into a quantity of water sufficient to make a fluid paste of them, squeeze out the mixture, filter the liquid obtained, and this liquid will contain the cerealine sufficiently pure to be studied in its effects. Its principal properties are: The liquid evaporated at a low temperature produces an amorphous, rough mass nearly colorless, and almost entirely soluble in distilled water; this solution coagulates between 158° and 167° Fah., and the coagulum is insoluble in acids and weak alkalies; the solution is precipitated by all diluted acids, by phosphoric acid at all the degrees of hydration, and even by a current of carbonic acid. All these precipitates redissolve with an excess of acid, sulphuric acid excepted. Concentrated sulphuric acid forms an insoluble downy white precipitate, and the concentrated vegetable acids, with the exception of tannic acid, do not determine any precipitate. Cerealine coagulated by an acid redissolves in an excess of the same acid, but it has become dead and has no more action on the starch. The alkalies do not form any precipitate, but they kill the cerealine as if it had been precipitated The neutral rennet does not make any precipitate in a solution of cerealine–5 centigrammes of dry cerealine transform in twenty-five minutes 10 grammes of starch, reduced to a paste by 100 grammes of water at 113° Fah. It will be seen that cerealine has a grand analogy with albumen and legumine, but it is distinguished from them by the action of the rennet, of the heat of acids, alcohol, and above all by its property of transforming the starch into glucose and dextrine.

It may be said that some albuminous substances have this property, but it must be borne in mind that these bodies, like gluten, for example, only possess it after the commencement of the decomposition. The albuminous matter approaching nearest to cerealine is the diastase, for it is only a transformation of the cerealine during the germination, the proof of which may be had in analyzing the embryous membrane, which shows more diastase and less cerealine in proportion to the advancement of the germination: it differs, however, from the diastase by the action of heat, alcohol, etc. It is seen that in every case the cerealine and the embryous membrane act together, and in an analogous manner; we shall shortly examine their effects on the digestion and in the phenomena of panification.

PHOSPHATE OF CALCIUM.–Mr. Payen was the first to make the observation that the greatest amount of phosphate of chalk is found in the teguments adjoining the farinaceous or floury mass. This observation is important from two points of view; in the first place, it shows us that this mineral aliment, necessary to the life of animals, is rejected from ordinary bread; and in the next place, it brings a new proof that phosphate of chalk is found, and ought to be found, in everyplace where there are membranes susceptible of exercising vital functions among animals as well as vegetables.

Phosphate of chalk is not in reality (as I wished to prove in another work) a plastic matter suitable for forming bones, for the bones of infants are three times more solid than those of old men, which contain three times as much of it. The quantity of phosphate of chalk necessary to the constitution of animals is in proportion to the temperature of those animals, and often in the inverse ratio of the weight of their bones, for vegetables, although they have no bones, require phosphate of chalk. This is because this salt is the natural stimulant of living membranes, and the bony tissue is only a depot of phosphate of chalk, analogous to the adipose tissue, the fat of which is absorbed when the alimentation coming from the exterior becomes insufficient. Now, as we know all the parts constituting the berry of wheat, it will be easy to explain the phenomena of panification, and to conclude from the present moment that it is not indifferent to reject from the bread this embryous membrane where the agents of digestion are found, viz., the phosphoric bodies and the phosphate of chalk.

THE ORIGIN OF NEW PROCESS MILLING

The following article was written by Albert Hoppin, editor of the Northwestern Miller, at the request of Special Agent Chas. W. Johnson, and forms a part of his report to the census bureau on the manufacturing industries of Minneapolis.

"The development of the milling industry in this city has been so intimately connected with the growth and prosperity of the city itself, that the steps by which the art of milling has reached its present high state of perfection are worthy of note, especially as Minneapolis may rightly claim the honor of having brought the improvements, which have within the last decade so thoroughly revolutionized the art of making flour, first into public notice, and of having contributed the largest share of capital and inventive skill to their full development. So much is this the case that the cluster of mills around the Falls of St. Anthony is to-day looked upon as the head-center of the milling industry not only of this country, but of the world. An exception to this broad statement may possibly be made in favor of the city of Buda Pest, in Austro-Hungary, from the leading mills in which the millers in this country have obtained many valuable ideas. To the credit of American millers and millwrights it must, however, be said that they have in all cases improved upon the information they have thus obtained.

"To rightly understand the change that has taken place in milling methods during the last ten years, it is necessary to compare the old way with the new, and to observe wherein they differ. From the days of Oliver Evans, the first American mechanic to make any improvement in milling machinery, until 1870, there was, if we may except some grain cleaning or smut machines, no very strongly marked advance in milling machinery or in the methods of manufacturing flour. It is true that the reel covered with finely-woven silk bolting cloth had taken the place of the muslin or woolen covered hand sieve, and that the old granite millstones have given place to the French burr; but these did not affect the essential parts of the modus operandi, although the quality of the product was, no doubt, materially improved. The processes employed in all the mills in the United States ten years ago were identical, or very nearly so, with those in use in the Brandywine Mills in Evans's day. They were very simple, and may be divided into two distinct operations.

"First. Grinding (literally) the wheat.

"Second. Bolting or separating the flour or interior portion of the berry from the outer husk, or bran. It may seem to some a rash assertion, but this primitive way of making flour is still in vogue in over one-half of the mills of the United States. This does not, however, affect the truth of the statement that the greater part of the flour now made in this country is made on an entirely different and vastly-improved system, which has come to be known to the trade as the new process.

"In looking for a reason for the sudden activity and spirit of progress which had its culmination in the new process, the character of the wheat raised in the different sections of the Union must be taken into consideration. Wheat may be divided into two classes, spring and winter, the latter generally being more starchy and easily pulverized, and at the same time having a very tough bran or husk, which does not readily crumble or cut to pieces in the process of grinding. It was with this wheat that the mills of the country had chiefly to do, and the defects of the old system of milling were not then so apparent. With the settlement of Minnesota, and the development of its capacities as a wheat-growing State, a new factor in the milling problem was introduced, which for a time bid fair to ruin every miller who undertook to solve it. The wheat raised in this State was, from the climatic conditions, a spring wheat, hard in structure and having a thin, tender, and friable bran. In milling this wheat, if an attempt was made to grind it as fine as was then customary to grind winter wheat, the bran was ground almost as fine as the flour, and passed as readily through the meshes of the bolting reels or sieves, rendering the flour dark, specky, and altogether unfit to enter the Eastern markets in competition with flour from the winter wheat sections. On the other hand, if the grinding was not so fine as to break up the bran, the interior of the berry being harder to pulverize, was not rendered sufficiently fine, and there remained after the flour was bolted out a large percentage of shorts or middlings, which, while containing the strongest and best flour in the berry, were so full of dirt and impurities as to render them unfit for any further grinding except for the very lowest grade of flour, technically known as 'red dog.' The flour produced from the first grinding was also more or less specky and discolored, and, in everything but strength, inferior to that made from winter wheat, while the 'yield' was so small, or, in other words, the amount of wheat which it took to make a barrel of flour was so large, that milling in Minnesota and other spring wheat sections was anything but profitable.

"The problem which ten years since confronted the millers of this city was how to obtain from the wheat which they had to grind a white, clear flour, and to so increase the yield as to leave some margin for profit. The first step in the solution of this problem was the invention by E. N. La Croix of the machine which has since been called the purifier, which removed the dirt and light impurities from the refuse middlings in the same manner that dust and chaff are removed from wheat by a fanning mill. The middlings thus purified were then reground, and the result was a much whiter and cleaner flour than it had been possible to obtain under the old process of low close grinding. This flour was called 'patent' or 'fancy,' and at once took a high position in the market. The first machine built by La Croix was immediately improved by George T. Smith, and has since then been the subject of numberless variations, changes, and improvements; and over the principles embodied in its construction there has been fought one of the longest and most bitter battles recorded in the annals of patent litigation in this country. The purifier is to-day the most important machine in use in the manufacture of flour in this country, and may with propriety be called the corner-stone of new process milling. The earliest experiments in its use in this country were made in what was then known as the 'big mill' in this city, owned by Washburn, Stephens & Co., and now known as the Washburn Mill B.

"The next step in the development of the new process, also originating in Minneapolis, was the abandonment of the old system of cracking the millstone, and substituting in its stead the use of smooth surfaces on the millstones, thus in a large measure doing away with the abrasion of the bran, and raising the quality of the flour produced at the first grinding. So far as we know, Mr. E. R. Stephens, a Minneapolis miller, then employed in the mill owned by Messrs. Pillsbury, Crocker & Fish, and now a member of the prominent milling firm of Freeman & Stephens, River Falls, Wisconsin, was the first to venture on this innovation. He also first practiced the widening of the furrows in the millstones and increasing their number, thus adding largely to the amount of middlings made at the first grinding, and raising the percentage of patent flour. He was warmly supported by Amasa K. Ostrander, since deceased, the founder and for a number of years the editor of the North-Western Miller, a trade newspaper. The new ideas were for a time vigorously combated by the millers, but their worth was so plain that they were soon adopted, not only in Minneapolis, but by progressive millers throughout the country. The truth was the 'new process' in its entirety, which may be summarized in four steps–first, grinding or, more properly, granulating the berry; second, bolting or separating the 'chop' or meal into first flour, middlings, and bran; third, purifying the middlings, fourth, regrinding and rebolting the middlings to produce the higher grade, or 'patent' flour. This higher grade flour drove the best winter wheat flours out of the Eastern markets, and placed milling in Minnesota upon a firm basis. The development of the 'new process' cannot be claimed by any one man. Hundreds of millers all over the country have contributed to its advance, but the millers of Minneapolis have always taken the lead.

"Within the past two or three years what may be distinctively called the 'new process' has, in the mills of Minneapolis and some few other leading mills in the country, been giving place to a new system, or rather, a refinement of the processes above described. This latest system is known to the trade as the 'gradual reduction' or high-grinding system, as the 'new process' is the medium high-grinding system, and the old way is the low or close grinding system. In using the gradual reduction in making flour the millstones are abandoned, except for finishing some of the inferior grades of flour, and the work is done by means of grooved and plain rollers, made of chilled iron or porcelain. In some cases disks of chilled iron, suitably furrowed, are used, and in others concave mills, consisting of a cylinder running against a concave plate. In Minneapolis the chilled iron rolls take the precedence of all other means.

"The system of gradual reduction is much more complicated than either of those which preceded it; but the results obtained are a marked advance over the 'new process.' The percentage of high-grade flour is increased, several grades of different degrees of excellence being produced, and the yield is also greater from a given quantity of wheat. The system consists in reducing the wheat to flour, not at one operation, as in the old system, nor in two grindings, as in the 'new process,' but in several successive reductions, four, five, or six, as the case may be. The wheat is first passed through a pair of corrugated chilled iron rollers, which merely split it open along the crease of the berry, liberating the dirt which lies in the crease so that it can be removed by bolting. A very small percentage of low-grade flour is also made in this reduction. After passing through what is technically called a 'scalping reel' to remove the dirt and flour, the broken wheat is passed through a second set of corrugated rollers, by which it is further broken up, and then passes through a second separating reel, which removes the flour and middlings. This operation is repeated successively until the flour portion of the berry is entirely removed from the bran, the necessary separation being made after each reduction. The middlings from the several reductions are passed through the purifiers, and, after being purified, are reduced to flour by successive reductions on smooth iron or porcelain rollers. In some cases, as stated above, iron disks and concave mills are substituted for the roller mill, but the operation is substantially the same. One of the principal objects sought to be attained by this high-grinding system is to avoid all abrasion of the bran, another is to take out the dirt in the crease of the berry at the beginning of the process, and still another to thoroughly free the bran from flour, so as to obtain as large a yield as possible. Incidental to the improved methods of milling, as now practiced in this country, is a marked improvement in the cleaning of the grain and preparing it for flouring. The earliest grain-cleaning machine was the 'smutter,' the office of which was to break the smut balls, and scour the outside of the bran to remove any adhering dust, the scouring machine being too harsh in its action, breaking the kernels of wheat, and so scratching and weakening the bran that it broke up readily in the grinding. The scouring process was therefore lessened, and was followed by brush machines, which brushed the dirt, loosened up and left by the scourer, from the berry. Other machines for removing the fuzzy and germ ends of the berry have also been introduced, and everything possible is done to free the grain from extraneous impurities before the process of reduction is commenced. In all the minor details of the mill there has been the same marked change, until the modern merchant mill of to-day no more resembles that of twenty-five years ago than does the modern cotton mill the old-fashioned distaff. The change has extended into the winter wheat sections, and no mill in the United States can hope to hold its place in the markets unless it is provided with the many improvements in machinery and processes which have resulted from the experiments begun in this city only ten years since, and which have made the name of Minneapolis and the products of her many mills famous throughout the world. The relative merits of the flour made by the new process and the old have been warmly discussed, but the general verdict of the great body of consumers is that the patent or new process flour is better in every way for bread making purposes, being clearer, whiter, more evenly granulated, and possessing more strength. Careful chemical analysis has confirmed this. As between winter and spring wheat flours made by the new process and gradual reduction systems, it maybe remarked that the former contain more starch and are whiter in color, while the latter, having more gluten, excel in strength. In milling all varieties of wheat, whether winter or spring, the new processes are in every way superior to the old, and, in aiding their inception and development, the millers of Minneapolis have conferred a lasting benefit on the country.

"Minneapolis, Minn., December 1, 1880."

THE MILLING STRUCTURES AND MACHINERY

Mr. Johnson added the following, showing the present status of the milling industry in Minneapolis:

"The description of the process of the manufacture of flour so well given above, conveys no idea of the extent and magnitude of the milling structures, machinery, and buildings employed in the business. Many of the leading millers and millwrights have personally visited and studied the best mills in England, France, Hungary, and Germany, and are as familiar with their theory, methods, and construction as of their own, and no expense or labor has been spared in introducing the most approved features of the improvements in the foreign mills. Experimenting is constantly going on, and the path behind the successful millers is strewn with the wrecks of failures. A very large proportion of the machinery is imported, though the American machinists are fast outstripping their European rivals in the quality and efficiency of the machinery needed for the new mills constantly going up.

"There are twenty-eight of these mills now constructed and at work, operating an equivalent of 412 runs of stone, consuming over sixteen million bushels of wheat, and manufacturing over three million barrels of flour annually. Their capacities range from 250 to 1,500 barrels of flour per day. Great as these capacities are, there is now one in process of construction, the Pillsbury A Mill, which at the beginning of the harvest of 1881 will have a capacity of 4,000 barrels daily. The Washburn A Mill, whose capacity is now 1,500 barrels, is being enlarged to make 8,500 barrels a day, and the Crown Roller Mill, owned by Christian Bros. & Co., is also being enlarged to produce 3,000 barrels a day. The largest mill in Europe has a daily capacity of but 2,800 barrels, and no European mill is fitted with the exquisite perfection of machinery and apparatus to be found in the mills of this city.

"The buildings are mainly built of blue limestone, found so abundant in the quarries of this city, range and line work, and rest on the solid ledge. The earlier built mills are severely plain, but the newer ones are greatly improved by the taste of the architect, and are imposing and beautiful in appearance."

DIRECT FOREIGN TRADE

The flour of Minneapolis, holding so high a rank in the markets of the world, is always in active demand, especially the best grades, and brings from $1.00 to $1.60 per barrel more than flour of the best qualities of southern, eastern, or foreign wheat. During the year nearly a million barrels were shipped direct to European and other foreign ports, on through bills of lading, and drawn for by banks here having special foreign exchange arrangements, at sight, on the day of shipment. This trade is constantly increasing, and the amount of flour handled by eastern commission men is decreasing in proportion.

Referring to the foregoing, the following letter from Mr. Geo. T. Smith to the editor of the London Miller is of interest:

SIR: I find published in the North-western Miller of December 24, 1880, extracts from an article on the origin of new process milling, prepared by Albert Hoppin, Esq., editor of the above-named journal, for the use of one of the statistical divisions of the United States census, which is so at variance, in at least one important particular, with the facts set forth in the paper read by me before the British and Irish millers, at their meeting in May last, that I think I ought to take notice of its statements, more especially as the North-Western Miller has quite a circulation on this side of the water.

As stated in the paper read by me above-mentioned, I was engaged in February, 1871, by Mr. Christian, who was then operating the "big," or Washburn Mill at Minneapolis, to take charge of the stones in that mill. At this time Mr. Christian was very much interested in the improvement of the quality of his flour, which in common with the flour of Minneapolis mills, without exception, was very poor indeed. For some time previous to this I had insisted to him most strenuously that the beginning of any improvement must be found in smooth, true, and well balanced stones, and it was because he was at last convinced that my ideas were at least worthy of a practical test I was placed in charge of his mill. Nearly two months were consumed in truing and smoothing the stone, as all millers in the mill had struck at once when they became acquainted with the character of the changes I proposed to make.

I remained with Mr. Christian until the latter part of 1871, in all about eight months. During this time the flour from the Washburn Mill attained a celebrity that made it known and sought after all over the United States. It commanded attention as an event of the very greatest importance, from the fact that it was justly felt that if a mill grinding spring wheat exclusively was capable of producing a flour infinitely superior in every way to the best that could be made from the finest varieties of winter wheats, the new North Western territory, with its peculiar adaptation to the growing of spring grain, and its boundless capacity for production, must at once become one of the most important sections of the country.

Mr. Christian's appreciation of the improvements I had made in his mill was attested by doubly-locked and guarded entrances, and by the stringent regulations which were adopted to prevent any of his employes carrying information with regard to the process to his competitors.

All this time other Minneapolis mills were doing such work and only such as they had done previously. Ought not the writer of an article on the origin of new process milling–which article is intended to become historical, and to have its authenticity indorsed by the government–to have known whether Mr. Christian, in the Washburn Mill, did or did not make a grade of flour which has hardly been excelled since for months before any other Minneapolis mill approached his product in any degree? And should he not be well enough acquainted with the milling of that period–1871-2–to know that such results as were obtained in the Washburn Mill could only be secured by the use of smooth and true stones? Mr. Stephens–whom I shall mention again presently–did not work in the Washburn Mill while I was in charge of it.